Ferrocene

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Ring Rotation in Ferrocene and Ferrocene-containing Polymers

Ferrocene is an organometallic molecular sandwich complex with an iron atom coordinated between two cyclopentadienyl rings. The reorientation of these rings in a process of rotational jump diffusion between multiple equilibrium sites on a circle is investigated using quasielastic neutron time of flight and backscattering spectroscopy experiments. Existing results on the ring rotation in bulk, c...

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(2,2-Dichloro­vinyl)ferrocene

The title compound, [Fe(C(5)H(5))(C(7)H(5)Cl(2))], represents a versatile building block for the preparation of π-conjugated redox-active compounds or polymetallic organometallic systems due to the presence of the electrochemically active ferrocenyl unit. It is therefore a potential starting material for the preperation of the corresponding alkyne. In the crystal, the alkenyl unit and the cyclo...

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Ferrocene-1-carbaldehyde thio­semi­carbazone

The asymmetric unit of the title compound, [Fe(C(5)H(5))(C(7)H(8)N(3)S)], consists of two crystallographically independent mol-ecules, A and B. The cyclo-penta-dienyl (Cp) rings in both mol-ecules adopt an eclipsed conformation and are parallel to each other, forming dihedral angles of 2.5 (3) and 1.1 (3)°, respectively. The mean plane of the semicarbazone group is coplanar with the attached Cp...

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1-(Bromo­mercurio)ferrocene

The asymmetric unit of the title compound, [Fe(C5H5)(C5H4BrHg)], contains two independent mol-ecules, A and B, in which the Hg-C bond lengths are 2.045 (6) and 2.046 (6) Å, the Hg-Br bond lengths are 2.4511 (9) and 2.4562 (7) Å, and the C-Hg-Br angles are 176.42 (17) and 177.32 (17)°. The two cyclo-penta-dienyl rings of mol-ecule A are eclipsed, while those of mol-ecule B are almost staggered. ...

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(1-Naphthyl­imino­meth­yl)ferrocene

In the title mol-ecule, [Fe(C(5)H(5))(C(16)H(12)N)], the cyclo-penta-dienyl rings are approximately eclipsed and the inter-planar angle is 0.8 (7)°. The Fe atom is slightly closer to the substituted cyclo-penta-dienyl ring, with an Fe⋯centroid distance of 1.639 (2) Å, compared with 1.645 (2) Å for the unsubstituted ring. The C=N double bond is essentially coplanar with the substituted cyclo-pen...

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ژورنال

عنوان ژورنال: Synlett

سال: 2015

ISSN: 0936-5214,1437-2096

DOI: 10.1055/s-0034-1381099